By Xue Duan, Lutz H. Gade, Gerard Parkin, Kenneth R. Poeppelmeier, Fraser Andrew Armstrong, Mikio Takano, David Michael P. Mingos
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Day, V. W,, Day, R. : J. Amer. Chem. Soc. 97, 2571 (1975). 123. F. : J. Chem. A 1971, 1797, 270l. 124. : J. Organomet. Chem. 88, C21 (1975). 125. : J. Organomet. Chem. 80, C53 (1974). 126. S. Dalton 1975, 1614. 127. F. , Jackson, W. , Matheson, T. : Chem. Cornrnun. 1974, 807. 128. S. Dalton 1973, 2589. 49 H. Vahrenkamp 129. 130. 131. 132. 133. 134. 135. 136. 137. 138. 139. 140. 141. 142. 143. 144. 145. 146. 147. 148. 149. 150. 151. 152. : Chem. Commun. 1972, 224. : J. Organomet. Chem. 42, C60 (1972).
Other simple Os 3 derivatives are the silicon- and germanium-bridged clusters [Me2EOs(CO)3]3 (E = Si, Ge), which are formed from silicon and germanium containing osmium carbonyls (55, 253), and which have structures like their ruthenium analog [50], and the nitrosyl-bridged Osa(CO)lo(NO)2 , which is chemically and structurally analogous to its ruthenium counterpart [49] (308). ".... ~Os(CO)3 (CO)30s. 66 H. . Os(CO)4 67 The substitution chemistry of triosmium carbonyls is extensive (153). Under mild conditions phosphines and arsines just replace CO ligands in Os3(CO)l 2 to form Osa(CO)12_nLn, where L is PPh 3 (50), PMe2Ph or AsMe2Ph (128, 129), PMe 3 or PEt 3 (132), and C4F4 (PPh 2)2 (f4 fos) (118).
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