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Extra info for Organic syntheses: An annual publication of satisfactory methods for the preparation of organic chemicals Organic synthesis). Volume XVI
Example text
62 (1997) 566a-5661. M. , Monitoring of a three step solid phase synthesis reaction involving a Heck reaction using magic angle spinning NMR spectroscopy, Tetrahedron, 52 phase organic reactions II: A review of the literature Nov 95Nov 96, Tetrahedron, 53 (1997) 5643-5678. 9. 8765-8770. , McLaren, EM. , Analytical techniques for combinatorial chemistry: Quantitative infrared spectroscopic measurements of deuteriumlabeled protecting groups, 1. Am. Chern. Soc. K. D. ), Annual Reports in Cornbinatorial Chernistry and Molecular Diversity, Vol.
Mol. , 3 (1997) 61-70. e. , Pittcon '97, Atlanta, March 1997. A, MacDonald, A. , In Proceedings of the International Society of Lab Automation and Robotics, 1996, pp. 336-348. , Matuszak, K, Searle, P. , Proceedings of the International Society of Lab Automation and Robotics, 1997, pp. 360-374. , ComTech '97, Frieberg, February 1997. , Yung, K, Shushan, B. , J. Chromatogr. A, 794, (1998) 3-13. , Raso, R. , Pittcon '97, Atlanta, March 1997. a. Perkin-Elmer Sciex Instruments, 71 Four Valley Drive, Concord, ON, Canada.
New flow probes and gradient technology make NMR more applicable in a high-throughput laboratory. 35 Chromatographic methods Considerable attention has been paid to the evaporative light-scattering detector (ELSD) [36] as a more universal HPLC detector than UV; in general it detects any analyte above a molecular weight of about 200 amu. However, the ELSD response is not linear and varies considerably between analogs of similar structure. These issues limit the usefulness of the ELSD for quantitative assessment of purity and yield.