By Andy I Bary; Craig George Cogger; Dan M Sullivan; Washington State University. Cooperative Extension.; Oregon State University. Extension Service.; All authors
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Transient recorders suitable for stopped-flow applications are available from only $1,000, and hence are very competitive with the storage oscilloscopes, which are generally used for semi-permanently recording the transient in analogue form. (For temperature-jump applications, due to the shorter sampling time required, the cost of the transient recorder is considerably higher). 3% can be achieved. The major factor limiting the accuracy appears to be the requirement of accurate volume delivery from the two drive-syringes.
On the area of the cell where the laser hits we have the monochromatic image of a high pressure Hg arc lamp with a very small spot dimension (HBO 100W/2 Osram). The light from the lamp goes through a high aperture quartz optics and a small monochromator (SPEX Minimatel: 4 aperture). 1 rom in max. size. e. extremely small. This condition limits the upper observable time by diffusion effects to about 1 ms. e. some 10- 8 sec); in fact we can do an accurate waveshape measurement of laser pulse, and reconstruct the signal by computer deconvolution.
Erth and H. Gerischer, Z. , ~, 629 (1967). F. ~. Crooks, J. Sci. , ~, 449 (1967). W. W. H. Turner and N. Sutin, J. Amer. Chern. , 21, 4130 (1970). F. W. B. A. Treg1oan, J. Phys. ,~, 349 (1973). F. W. S. Faraday 1, 69, 1648 (1973). E. H. Robinson, Trans. , 67, 1707 -(1971). M. C. Greenhow, Chern. PhIS. , ~, 583, (1971). J. Ivin, R. J. McGarvey, J. Amer. Chern. , ~, 1763 (1972). N. Sutin and C. Creutz, J. Amer. Chern. 2, 7177 (1973). E:F. E. H. Robinson, J. Phys. , Sci. ,~, 165 (1971). R. -Jost and L.