By C. F. Van Sumere, W. Van Brussel, K. Vante Casteele (auth.), Tony Swain, Jeffrey B. Harbone, Chris F. Van Sumere (eds.)
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Il: 449. Kingsbury, C. , J. H. Looker. 1975. J. Org. Chem. , Y. Terui, K. Tori, N. Tsuji. 1976. Tetrahedron Letters 8: 619.
8) of methyl lividate clearly shows a 3JCH interaction between the side chain methylene protons and C-5. The resonance for the latter appears, therefore, as a doublet of triplets corroborating the formulation (XIX) as the correct one to represent hydroxy physodic acid itself. By far the most important use of 13C_NMR for the is in the elucidation of biosynthetic pathways 3-5. By feeding appropriately 13C enriched precursors and follow up of the metabolite by NMR clearly pinpoints biocgem~st 0 HO 0 OH 0 OH OH 0 HO Q'CO'CH 3 0H (XXIX) 0 It HO Versiconal Acetate OH ~CO J OH Figure 8.
Neszm elyi, H. Wagner. 1977. Proceedin gs of the V Hunga rian Biofla vonoid Symposium. Akademiai Kiado -Elsev ier, Budap est and Amsterdam, in press. Chen, Y. , R. Liu, H. -Yo Hsu, S. Yamamura, Y. Shizu ri, Y. Hirata . 1977. Bull. Chem. Soc. Japan 50: 1824. Cocke rill, A. , G. L. O. Davies , R. C. Harden , D. Rackham. 1973. Chem. Rev. 73: 553. Cox, R. , F. Churc hill, R. J. Cole:- J. W. Dorne r. 1977. J. Am. Chem. Soc. 99: 9: 3159. , G. W. Kilbee , D. ~ Whitin g. 1974. J. C. S. Perkin I 1497. Cussan s, N.